Laser Ablation Inductively Coupled Plasma Atomic Emission
Spectrometry for Soil Analysis

D 2005

Laser Ablation Inductively Coupled Plasma Atomic Emission Spectrometry for Soil Analysis

HOLÁ, Markéta, Pavel KRÁSENSKÝ a Viktor KANICKÝ

Základní údaje

Originální název

Laser Ablation Inductively Coupled Plasma Atomic Emission Spectrometry for Soil Analysis

Název česky

ICP-OES pro analýzu půd

Autoři

HOLÁ, Markéta (203 Česká republika, garant), Pavel KRÁSENSKÝ (203 Česká republika) a Viktor KANICKÝ (203 Česká republika)

Vydání

Pardubice, International Conference on Inorganic Environmental Analysis - Proceedings of the 4th Conference, od s. 88-90, 3 s. 2005

Nakladatel

Spektroskopická společnost J.M.Marci, Univerzita Pardubice

Další údaje

Jazyk

angličtina

Typ výsledku

Stať ve sborníku

Obor

10406 Analytical chemistry

Stát vydavatele

Česká republika

Utajení

není předmětem státního či obchodního tajemství

Kód RIV

RIV/00216224:14310/05:00014698

Organizační jednotka

Přírodovědecká fakulta

Klíčová slova anglicky

Laser ablation; Indctively coupled plasma; Optical emission spectrometry; Soil

Štítky

Indctively coupled plasma, laser ablation, Optical emission spectrometry, soil

Změněno: 3. 2. 2006 16:16, Mgr. Markéta Holá, Ph.D.

Anotace

ORIG CZ

V originále

Analysis of soils is very important in environmental and agricultural chemistry. The conventional methods of soil preparation for inductively coupled plasma optical emission spectrometry (ICP-OES) are based on sample dissolution. However, decomposition of some samples is a very complicated and time-consuming procedure. Therefore, ICP spectrometry combined with laser ablation (LA) might be a solution for the analysis of resistant materials such as soils or other geological samples. Soil samples were presented for the analysis as cast pellets with epoxide resin binder. Q-switched Nd:YAG laser operated at the wavelengths of 1064 nm and 266 nm and repetition rate of 10 Hz was used for ablation of prepared pellets. Samples were placed into an ablation cell which was connected with XY-translator allowing a sample moving during ablation. The ablated material was transported by Ar along a polyamide tubing to ICP spectrometer Jobin Yvon 170 Ultrace (laterally viewed). The analytical response for soil pellets were used to produce the signal vs. element content plots using 1064 nm and 266 nm laser wavelenght.

Česky

Byla vypracována metoda pro stanovení vybraných stopových prvků v zemědělských půdách technikou LA-ICP-OES.

Návaznosti

MSM0021622412, záměr

Název: Interakce mezi chemickými látkami, prostředím a biologickými systémy a jejich důsledky na globální, regionální a lokální úrovni (INCHEMBIOL) (Akronym: INCHEMBIOL)

Investor: Ministerstvo školství, mládeže a tělovýchovy ČR, Interakce mezi chemickými látkami, prostředím a biologickými systémy a jejich důsledky na globální , regionální a lokální úrovni

Citovat

HOLÁ, Markéta, Pavel KRÁSENSKÝ a Viktor KANICKÝ. Laser Ablation Inductively Coupled Plasma Atomic Emission Spectrometry for Soil Analysis. In International Conference on Inorganic Environmental Analysis - Proceedings of the 4th Conference. Pardubice: Spektroskopická společnost J.M.Marci, Univerzita Pardubice, 2005, s. 88-90.

@inproceedings{619225,
   author = {Holá, Markéta and Krásenský, Pavel and Kanický, Viktor},
   address = {Pardubice},
   booktitle = {International Conference on Inorganic Environmental Analysis - Proceedings of the 4th Conference},
   keywords = {Laser ablation; Indctively coupled plasma; Optical emission spectrometry; Soil},
   language = {eng},
   location = {Pardubice},
   pages = {88-90},
   publisher = {Spektroskopická společnost J.M.Marci, Univerzita Pardubice},
   title = {Laser Ablation Inductively Coupled Plasma Atomic Emission Spectrometry for Soil Analysis},
   year = {2005}
}

TY  - JOUR
ID  - 619225
AU  - Holá, Markéta - Krásenský, Pavel - Kanický, Viktor
PY  - 2005
TI  - Laser Ablation Inductively Coupled Plasma Atomic Emission Spectrometry for Soil Analysis
PB  - Spektroskopická společnost J.M.Marci, Univerzita Pardubice
CY  - Pardubice
KW  - Laser ablation
KW  - Indctively coupled plasma
KW  - Optical emission spectrometry
KW  - Soil
N2  - Analysis of soils is very important in environmental and agricultural chemistry. The conventional methods of soil preparation for inductively coupled plasma optical emission spectrometry (ICP-OES) are based on sample dissolution. However, decomposition of some samples is a very complicated and time-consuming procedure. Therefore, ICP spectrometry combined with laser ablation (LA) might be a solution for the analysis of resistant materials such as soils or other geological samples. Soil samples were presented for the analysis as cast pellets with epoxide resin binder. Q-switched Nd:YAG laser operated at the wavelengths of 1064 nm and 266 nm and repetition rate of 10 Hz was used for ablation of prepared pellets. Samples were placed into an ablation cell which was connected with XY-translator allowing a sample moving during ablation. The ablated material was transported by Ar along a polyamide tubing to ICP spectrometer Jobin Yvon 170 Ultrace (laterally viewed). The analytical response for soil pellets were used to produce the signal vs. element content plots using 1064 nm and 266 nm laser wavelenght.
ER  -

HOLÁ, Markéta, Pavel KRÁSENSKÝ a Viktor KANICKÝ. Laser Ablation Inductively Coupled Plasma Atomic Emission Spectrometry for Soil Analysis. In \textit{International Conference on Inorganic Environmental Analysis - Proceedings of the 4th Conference}. Pardubice: Spektroskopická společnost J.M.Marci, Univerzita Pardubice, 2005, s.~88-90.

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