Sol-gel preparation and characterization of gadolinium
aluminate

J 2007

Sol-gel preparation and characterization of gadolinium aluminate

CIZAUSKAITE, Sigute, Vendula REICHLOVÁ, Giedre NENARTAVICIENE, Aldona BEGANSKIENE, Jiří PINKAS et. al.

Základní údaje

Originální název

Sol-gel preparation and characterization of gadolinium aluminate

Název česky

Sol-gel příprava a charakterizace oxidů gadolinito-hlinitých

Autoři

CIZAUSKAITE, Sigute (440 Litva), Vendula REICHLOVÁ (203 Česká republika), Giedre NENARTAVICIENE (440 Litva), Aldona BEGANSKIENE (440 Litva), Jiří PINKAS (203 Česká republika, garant) a Aivaras KAREIVA (440 Litva)

Vydání

Materials Chemistry and Physics, Elsevier, 2007, 0254-0584

Další údaje

Jazyk

angličtina

Typ výsledku

Článek v odborném periodiku

Obor

10402 Inorganic and nuclear chemistry

Stát vydavatele

Nizozemské království

Utajení

není předmětem státního či obchodního tajemství

Impakt faktor

Impact factor: 1.871

Kód RIV

RIV/00216224:14310/07:00021994

Organizační jednotka

Přírodovědecká fakulta

UT WoS

000245044500018

Klíčová slova anglicky

Ceramics; Electronic materials; Chemical synthesis; Sol-gel growth

Štítky

ceramics, Chemical synthesis, Electronic materials, Sol-gel growth

Příznaky

Mezinárodní význam, Recenzováno

Změněno: 31. 5. 2009 22:21, prof. RNDr. Jiří Pinkas, Ph.D.

Anotace

ORIG CZ

V originále

This paper reports on the results concerning the sol-gel preparation of nanocrystalline gadolinium aluminate (GdAlO3, GAP) using different starting materials. The gadolinium nitrate or gadolinium oxide as Gd raw compounds and aluminium nitrate as Al source were used in the sol-gel processing. The metal ions, generated by dissolving starting materials of metals in the diluted acetic acid were complexed by 1,2-ethanediol to obtain the precursor for the GAP. The phase transformations, composition and micro-structural features in the gels and polycrystalline samples were studied by thermal analysis (TGA/DTA), powder X-ray diffraction analysis (XRD), infrared spectroscopy (IR) and scanning electron microscopy (SEM). The XRD patterns of the GAP ceramic sintered at 1000 oC using gadolinium oxide as starting material were identical with the single-phase perovskite GdAlO3 composition.

Česky

Sol-gel příprava a charakterizace oxidů gadolinito-hlinitých.

Návaznosti

MSM0021622410, záměr

Název: Fyzikální a chemické vlastnosti pokročilých materiálů a struktur

Investor: Ministerstvo školství, mládeže a tělovýchovy ČR, Fyzikální a chemické vlastnosti pokročilých materiálů a struktur

Citovat

CIZAUSKAITE, Sigute, Vendula REICHLOVÁ, Giedre NENARTAVICIENE, Aldona BEGANSKIENE, Jiří PINKAS a Aivaras KAREIVA. Sol-gel preparation and characterization of gadolinium aluminate. Materials Chemistry and Physics. Elsevier, 2007, roč. 102, č. 1, s. 105-110. ISSN 0254-0584.

@article{715471,
   author = {Cizauskaite, Sigute and Reichlová, Vendula and Nenartaviciene, Giedre and Beganskiene, Aldona and Pinkas, Jiří and Kareiva, Aivaras},
   article_number = {1},
   keywords = {Ceramics; Electronic materials; Chemical synthesis; Sol-gel growth},
   language = {eng},
   issn = {0254-0584},
   journal = {Materials Chemistry and Physics},
   title = {Sol-gel preparation and characterization of gadolinium aluminate},
   volume = {102},
   year = {2007}
}

TY  - JOUR
ID  - 715471
AU  - Cizauskaite, Sigute - Reichlová, Vendula - Nenartaviciene, Giedre - Beganskiene, Aldona - Pinkas, Jiří - Kareiva, Aivaras
PY  - 2007
TI  - Sol-gel preparation and characterization of gadolinium aluminate
JF  - Materials Chemistry and Physics
VL  - 102
IS  - 1
SP  - 105-110
EP  - 105-110
PB  - Elsevier
SN  - 02540584
KW  - Ceramics
KW  - Electronic materials
KW  - Chemical synthesis
KW  - Sol-gel growth
N2  - This paper reports on the results concerning the sol-gel preparation of nanocrystalline gadolinium aluminate (GdAlO3, GAP) using different starting materials. The gadolinium nitrate or gadolinium oxide as Gd raw compounds and aluminium nitrate as Al source were used in the sol-gel processing. The metal ions, generated by dissolving starting materials of metals in the diluted acetic acid were complexed by 1,2-ethanediol to obtain the precursor for the GAP. The phase transformations, composition and micro-structural features in the gels and polycrystalline samples were studied by thermal analysis (TGA/DTA), powder X-ray diffraction analysis (XRD), infrared spectroscopy (IR) and scanning electron microscopy (SEM). The XRD patterns of the GAP ceramic sintered at 1000 oC using gadolinium oxide as starting material were identical with the single-phase perovskite GdAlO3 composition.
ER  -

CIZAUSKAITE, Sigute, Vendula REICHLOVÁ, Giedre NENARTAVICIENE, Aldona BEGANSKIENE, Jiří PINKAS a Aivaras KAREIVA. Sol-gel preparation and characterization of gadolinium aluminate. \textit{Materials Chemistry and Physics}. Elsevier, 2007, roč.~102, č.~1, s.~105-110. ISSN~0254-0584.

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