Comparison of LA-ICP-MS and LA-ICP-OES for the analysis of some
elements in fly ashes

J 2011

Comparison of LA-ICP-MS and LA-ICP-OES for the analysis of some elements in fly ashes

STAŇKOVÁ, Alice; Nicole GILON; Lionel DUTRUCH a Viktor KANICKÝ

Základní údaje

Originální název

Comparison of LA-ICP-MS and LA-ICP-OES for the analysis of some elements in fly ashes

Autoři

STAŇKOVÁ, Alice; Nicole GILON; Lionel DUTRUCH a Viktor KANICKÝ

Vydání

Journal of Analytical Atomic Spectrometry, Cambridge, Royal Society of Chemistry, 2011, 0267-9477

Další údaje

Jazyk

angličtina

Typ výsledku

Článek v odborném periodiku

Obor

10406 Analytical chemistry

Stát vydavatele

Spojené státy

Utajení

není předmětem státního či obchodního tajemství

Odkazy

URL

Impakt faktor

Impact factor: 3.220

Označené pro přenos do RIV

Ano

Kód RIV

RIV/00216224:14310/11:00055726

Organizační jednotka

Přírodovědecká fakulta

DOI

https://doi.org/10.1039/c0ja00020e

UT WoS

000286613700023

Klíčová slova anglicky

analysis elements LA-ICP-MS

Změněno: 20. 4. 2012 12:11, Ing. Andrea Mikešková

Anotace

V originále

In this work quantitative analysis of minor and trace elements in fly ash by nanosecond laser ablation (LA)-ICP-MS and LA-ICP-OES was investigated in terms of detection limits and accuracy. Different binders and modifiers (silver or chromophores) were added to the fly ash powder to prepare mechanically stable pellets and improve sensitivity (signal to concentration ratio). Maleic acid was found to provide a higher degree of homogeneity between sensitivities across the different fly ashes tested. Ashes were from different origins: domestic waste incinerator or ashes from various coal-fired power plants. A calibration procedure using reference materials as standards was employed, the LAICP- MS analysis gave an acceptable accuracy (estimated from NIST 1633), better results were obtained using fused bead preparation.

Návaznosti

MSM0021622411, záměr

Název: Studium a aplikace plazmochemických reakcí v neizotermickém nízkoteplotním plazmatu a jeho interakcí s povrchem pevných látek

Investor: Ministerstvo školství, mládeže a tělovýchovy ČR, Studium a aplikace plazmochemických reakcí v neizotermickém nízkoteplotním plazmatu a jeho interakcí s povrchem pevných látek

Citovat

STAŇKOVÁ, Alice; Nicole GILON; Lionel DUTRUCH a Viktor KANICKÝ. Comparison of LA-ICP-MS and LA-ICP-OES for the analysis of some elements in fly ashes. Journal of Analytical Atomic Spectrometry. Cambridge: Royal Society of Chemistry, 2011, roč. 26, č. 2, s. 443–449. ISSN 0267-9477. Dostupné z: https://doi.org/10.1039/c0ja00020e.

@article{972462,
   author = {Staňková, Alice and Gilon, Nicole and Dutruch, Lionel and Kanický, Viktor},
   article_location = {Cambridge},
   article_number = {2},
   doi = {https://doi.org/10.1039/c0ja00020e},
   keywords = {analysis elements LA-ICP-MS},
   language = {eng},
   issn = {0267-9477},
   journal = {Journal of Analytical Atomic Spectrometry},
   title = {Comparison of LA-ICP-MS and LA-ICP-OES for the analysis of some elements in fly ashes},
   url = {http://pubs.rsc.org/en/Content/ArticleLanding/2011/JA/c0ja00020e},
   volume = {26},
   year = {2011}
}

TY  - JOUR
ID  - 972462
AU  - Staňková, Alice - Gilon, Nicole - Dutruch, Lionel - Kanický, Viktor
PY  - 2011
TI  - Comparison of LA-ICP-MS and LA-ICP-OES for the analysis of some elements in fly ashes
JF  - Journal of Analytical Atomic Spectrometry
VL  - 26
IS  - 2
SP  - 443–449
EP  - 443–449
PB  - Royal Society of Chemistry
SN  - 02679477
KW  - analysis elements LA-ICP-MS
UR  - http://pubs.rsc.org/en/Content/ArticleLanding/2011/JA/c0ja00020e
L2  - http://pubs.rsc.org/en/Content/ArticleLanding/2011/JA/c0ja00020e
N2  - In this work quantitative analysis of minor and trace elements in fly ash by nanosecond laser ablation (LA)-ICP-MS and LA-ICP-OES was investigated in terms of detection limits and accuracy. Different binders and modifiers (silver or chromophores) were added to the fly ash powder to prepare mechanically stable pellets and improve sensitivity (signal to concentration ratio). Maleic acid was found to provide a higher degree of homogeneity between sensitivities across the different fly ashes tested. Ashes were from different origins: domestic waste incinerator or ashes from various coal-fired power plants. A calibration procedure using reference materials as standards was employed, the LAICP- MS analysis gave an acceptable accuracy (estimated from NIST 1633), better results were obtained using fused bead preparation.
ER  -

STAŇKOVÁ, Alice; Nicole GILON; Lionel DUTRUCH a Viktor KANICKÝ. Comparison of LA-ICP-MS and LA-ICP-OES for the analysis of some elements in fly ashes. \textit{Journal of Analytical Atomic Spectrometry}. Cambridge: Royal Society of Chemistry, 2011, roč.~26, č.~2, s.~443–449. ISSN~0267-9477. Dostupné z: https://doi.org/10.1039/c0ja00020e.

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