Course Information

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Mgr. Aleš Stýskalík, Ph.D. (seminar tutor)
Jaroslav Keller (assistant)
RNDr. Mgr. Iveta Třísková, Ph.D. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

The course “Chemical synthesis – laboratory“ represents an elementary laboratory course of preparatory chemistry in bachelor’s studies and aims for deepening and adopting fundamental as well as complementary techniques used in synthetic organic and inorganic chemistry (e.g. vacuum distillation, work under lowered temperatures, column chromatography, synthesis in waterless environment, …) including selected physico-chemical methods for identification of products (determining melting point and refractive index, gas chromatography, IR spectroscopy). Exercises are chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.

Learning outcomes

By the end of this course, students:
- will have mastered elementary and complementary techniques commonly used in inorganic and organic synthesis.
- will be capable of handling laboratory equipment necessary for analysis of purity and identification of prepared solutions with ease (gas chromatograph, IR spectrometer, refractometer, melting point apparatus and others).
- will have built self-confidence and gained manual skillfulness essential for work in chemical laboratory.
- will be able to explain chemical nature of selected preparatory techniques. Exercises were chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.
- will have learnt to report thoroughly on outcomes of their work and will have mastered basic chemical calculations needed for their laboratory praxis.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of benzophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practiced on the real inorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Mgr. Aleš Stýskalík, Ph.D. (seminar tutor)
Jaroslav Keller (assistant)
RNDr. Mgr. Iveta Třísková, Ph.D. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Mon 19. 2. to Sun 26. 5. Mon 10:00–17:50 C10/109, J. Literák, Z. Moravec
C2200/03: Mon 19. 2. to Sun 26. 5. Thu 7:00–14:50 C10/109, S. Janků, A. Stýskalík
C2200/04: Mon 19. 2. to Sun 26. 5. Thu 7:00–14:50 C10/109, S. Janků, A. Stýskalík

Prerequisites

C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 38/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

The course “Chemical synthesis – laboratory“ represents an elementary laboratory course of preparatory chemistry in bachelor’s studies and aims for deepening and adopting fundamental as well as complementary techniques used in synthetic organic and inorganic chemistry (e.g. vacuum distillation, work under lowered temperatures, column chromatography, synthesis in waterless environment, …) including selected physico-chemical methods for identification of products (determining melting point and refractive index, gas chromatography, IR spectroscopy). Exercises are chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.

Learning outcomes

By the end of this course, students:
- will have mastered elementary and complementary techniques commonly used in inorganic and organic synthesis.
- will be capable of handling laboratory equipment necessary for analysis of purity and identification of prepared solutions with ease (gas chromatograph, IR spectrometer, refractometer, melting point apparatus and others).
- will have built self-confidence and gained manual skillfulness essential for work in chemical laboratory.
- will be able to explain chemical nature of selected preparatory techniques. Exercises were chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.
- will have learnt to report thoroughly on outcomes of their work and will have mastered basic chemical calculations needed for their laboratory praxis.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of benzophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practiced on the real inorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Jaroslav Dorošenko, Ph.D. (seminar tutor)
RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Mgr. Jan Badin (assistant)
Jaroslav Keller (assistant)
Mgr. Jakub Martikan (assistant)
Ing. Michaela Šusterová (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Mon 8:00–15:50 C10/109, J. Dorošenko, S. Janků
C2200/02: Mon 8:00–15:50 C10/109, J. Dorošenko, S. Janků
C2200/03: Thu 8:00–15:50 C10/109, J. Literák, Z. Moravec

Prerequisites

( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika || C4221 Biochemical Lab Technique )&&( C1020 General Chemistry || C1601 General and Inorg. Chemistry )
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 14/120, only registered: 0/120

fields of study / plans the course is directly associated with

there are 7 fields of study the course is directly associated with, display

Course objectives

The course “Chemical synthesis – laboratory“ represents an elementary laboratory course of preparatory chemistry in bachelor’s studies and aims for deepening and adopting fundamental as well as complementary techniques used in synthetic organic and inorganic chemistry (e.g. vacuum distillation, work under lowered temperatures, column chromatography, synthesis in waterless environment, …) including selected physico-chemical methods for identification of products (determining melting point and refractive index, gas chromatography, IR spectroscopy). Exercises are chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.

Learning outcomes

By the end of this course, students:
- will have mastered elementary and complementary techniques commonly used in inorganic and organic synthesis.
- will be capable of handling laboratory equipment necessary for analysis of purity and identification of prepared solutions with ease (gas chromatograph, IR spectrometer, refractometer, melting point apparatus and others).
- will have built self-confidence and gained manual skillfulness essential for work in chemical laboratory.
- will be able to explain chemical nature of selected preparatory techniques. Exercises were chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.
- will have learnt to report thoroughly on outcomes of their work and will have mastered basic chemical calculations needed for their laboratory praxis.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Jaroslav Dorošenko, Ph.D. (seminar tutor)
RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Jaroslav Keller (assistant)
Mgr. Lucie Leonová (assistant)
Mgr. David Majer (assistant)
Mgr. Jakub Nagy (assistant)
Ing. Michaela Šusterová (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Wed 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/02: Wed 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/03: Mon 12:00–19:50 C10/109, J. Dorošenko, J. Literák
C2200/04: Mon 12:00–19:50 C10/109, J. Dorošenko, J. Literák

Prerequisites

C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 21/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

The course “Chemical synthesis – laboratory“ represents an elementary laboratory course of preparatory chemistry in bachelor’s studies and aims for deepening and adopting fundamental as well as complementary techniques used in synthetic organic and inorganic chemistry (e.g. vacuum distillation, work under lowered temperatures, column chromatography, synthesis in waterless environment, …) including selected physico-chemical methods for identification of products (determining melting point and refractive index, gas chromatography, IR spectroscopy). Exercises are chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.

Learning outcomes

By the end of this course, students:
- will have mastered elementary and complementary techniques commonly used in inorganic and organic synthesis.
- will be capable of handling laboratory equipment necessary for analysis of purity and identification of prepared solutions with ease (gas chromatograph, IR spectrometer, refractometer, melting point apparatus and others).
- will have built self-confidence and gained manual skillfulness essential for work in chemical laboratory.
- will be able to explain chemical nature of selected preparatory techniques. Exercises were chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.
- will have learnt to report thoroughly on outcomes of their work and will have mastered basic chemical calculations needed for their laboratory praxis.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of benzophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practiced on the real inorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Jaroslav Dorošenko, Ph.D. (seminar tutor)
RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Jaroslav Keller (assistant)
Mgr. Lucie Leonová (assistant)
Mgr. Michal Mlynek (assistant)
Mgr. Tomáš Pokorný (assistant)
Mgr. Lukáš Veselý (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Wed 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/02: Wed 8:00–15:50 C10/109, J. Dorošenko, S. Janků
C2200/03: Thu 8:00–15:50 C10/109, J. Dorošenko, J. Literák

Prerequisites

( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika || C4221 Biochemical Lab Technique )&&( C1020 General Chemistry || C1601 General and Inorg. Chemistry )
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 10/120, only registered: 3/120

fields of study / plans the course is directly associated with

there are 7 fields of study the course is directly associated with, display

Course objectives

The course “Chemical synthesis – laboratory“ represents an elementary laboratory course of preparatory chemistry in bachelor’s studies and aims for deepening and adopting fundamental as well as complementary techniques used in synthetic organic and inorganic chemistry (e.g. vacuum distillation, work under lowered temperatures, column chromatography, synthesis in waterless environment, …) including selected physico-chemical methods for identification of products (determining melting point and refractive index, gas chromatography, IR spectroscopy). Exercises are chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.

Learning outcomes

By the end of this course, students:
- will have mastered elementary and complementary techniques commonly used in inorganic and organic synthesis.
- will be capable of handling laboratory equipment necessary for analysis of purity and identification of prepared solutions with ease (gas chromatograph, IR spectrometer, refractometer, melting point apparatus and others).
- will have built self-confidence and gained manual skillfulness essential for work in chemical laboratory.
- will be able to explain chemical nature of selected preparatory techniques. Exercises were chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.
- will have learnt to report thoroughly on outcomes of their work and will have mastered basic chemical calculations needed for their laboratory praxis.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Jaroslav Dorošenko, Ph.D. (seminar tutor)
RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Mgr. Lucie Leonová (assistant)
Mgr. Michal Mlynek (assistant)
Mgr. Jakub Nagy (assistant)
Mgr. Tomáš Pokorný (assistant)
Mgr. Lukáš Veselý (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Thu 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/02: Thu 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/03: Mon 8:00–15:50 C10/109, J. Dorošenko, J. Literák
C2200/04: Mon 8:00–15:50 C10/109, J. Dorošenko, J. Literák

Prerequisites

C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 1/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

The course “Chemical synthesis – laboratory“ represents an elementary laboratory course of preparatory chemistry in bachelor’s studies and aims for deepening and adopting fundamental as well as complementary techniques used in synthetic organic and inorganic chemistry (e.g. vacuum distillation, work under lowered temperatures, column chromatography, synthesis in waterless environment, …) including selected physico-chemical methods for identification of products (determining melting point and refractive index, gas chromatography, IR spectroscopy). Exercises are chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.

Learning outcomes

By the end of this course, students:
- will have mastered elementary and complementary techniques commonly used in inorganic and organic synthesis.
- will be capable of handling laboratory equipment necessary for analysis of purity and identification of prepared solutions with ease (gas chromatograph, IR spectrometer, refractometer, melting point apparatus and others).
- will have built self-confidence and gained manual skillfulness essential for work in chemical laboratory.
- will be able to explain chemical nature of selected preparatory techniques. Exercises were chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.
- will have learnt to report thoroughly on outcomes of their work and will have mastered basic chemical calculations needed for their laboratory praxis.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of benzophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practiced on the real inorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Jaroslav Dorošenko, Ph.D. (seminar tutor)
RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Mgr. Aleš Stýskalík, Ph.D. (seminar tutor)
Mgr. Ondřej Czechaczek (assistant)
Mgr. Michal Mlynek (assistant)
Mgr. Tomáš Pokorný (assistant)
Mgr. Adam Štefek (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Wed 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/02: Wed 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/03: Thu 8:00–15:50 C10/109, J. Dorošenko, J. Literák
C2200/04: Thu 8:00–15:50 C10/109, J. Dorošenko, J. Literák

Prerequisites

( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika || C4221 Biochemical Lab Technique )&&( C1020 General Chemistry || C1601 General and Inorg. Chemistry )
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 1/120

fields of study / plans the course is directly associated with

there are 7 fields of study the course is directly associated with, display

Course objectives

The course “Chemical synthesis – laboratory“ represents an elementary laboratory course of preparatory chemistry in bachelor’s studies and aims for deepening and adopting fundamental as well as complementary techniques used in synthetic organic and inorganic chemistry (e.g. vacuum distillation, work under lowered temperatures, column chromatography, synthesis in waterless environment, …) including selected physico-chemical methods for identification of products (determining melting point and refractive index, gas chromatography, IR spectroscopy). Exercises are chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.

Learning outcomes

By the end of this course, students:
- will have mastered elementary and complementary techniques commonly used in inorganic and organic synthesis.
- will be capable of handling laboratory equipment necessary for analysis of purity and identification of prepared solutions with ease (gas chromatograph, IR spectrometer, refractometer, melting point apparatus and others).
- will have built self-confidence and gained manual skillfulness essential for work in chemical laboratory.
- will be able to explain chemical nature of selected preparatory techniques. Exercises were chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.
- will have learnt to report thoroughly on outcomes of their work and will have mastered basic chemical calculations needed for their laboratory praxis.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Mgr. Aleš Stýskalík, Ph.D. (seminar tutor)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

The course “Chemical synthesis – laboratory“ represents an elementary laboratory course of preparatory chemistry in bachelor’s studies and aims for deepening and adopting fundamental as well as complementary techniques used in synthetic organic and inorganic chemistry (e.g. vacuum distillation, work under lowered temperatures, column chromatography, synthesis in waterless environment, …) including selected physico-chemical methods for identification of products (determining melting point and refractive index, gas chromatography, IR spectroscopy). Exercises are chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.

Learning outcomes

By the end of this course, students:
- will have mastered elementary and complementary techniques commonly used in inorganic and organic synthesis.
- will be capable of handling laboratory equipment necessary for analysis of purity and identification of prepared solutions with ease (gas chromatograph, IR spectrometer, refractometer, melting point apparatus and others).
- will have built self-confidence and gained manual skillfulness essential for work in chemical laboratory.
- will be able to explain chemical nature of selected preparatory techniques. Exercises were chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.
- will have learnt to report thoroughly on outcomes of their work and will have mastered basic chemical calculations needed for their laboratory praxis.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of benzophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practiced on the real inorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Mgr. Aleš Stýskalík, Ph.D. (seminar tutor)
Mgr. Ondřej Czechaczek (assistant)
Mgr. Lubomír Havlíček (assistant)
Mgr. Martin Kejík, Ph.D. (assistant)
Ing. Antonín Račický, Ph.D. (assistant)
Mgr. Michal Žalud, Ph.D. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Wed 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/02: Wed 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/03: Thu 8:00–15:50 C10/109, J. Literák, A. Stýskalík
C2200/04: Thu 8:00–15:50 C10/109, J. Literák, A. Stýskalík

Prerequisites

( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika || C4221 Biochemical Lab Technique )&&( C1020 General Chemistry || C1601 General and Inorg. Chemistry )
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120

fields of study / plans the course is directly associated with

there are 7 fields of study the course is directly associated with, display

Course objectives

The course “Chemical synthesis – laboratory“ represents an elementary laboratory course of preparatory chemistry in bachelor’s studies and aims for deepening and adopting fundamental as well as complementary techniques used in synthetic organic and inorganic chemistry (e.g. vacuum distillation, work under lowered temperatures, column chromatography, synthesis in waterless environment, …) including selected physico-chemical methods for identification of products (determining melting point and refractive index, gas chromatography, IR spectroscopy). Exercises are chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.

Learning outcomes

By the end of this course, students:
- will have mastered elementary and complementary techniques commonly used in inorganic and organic synthesis.
- will be capable of handling laboratory equipment necessary for analysis of purity and identification of prepared solutions with ease (gas chromatograph, IR spectrometer, refractometer, melting point apparatus and others).
- will have built self-confidence and gained manual skillfulness essential for work in chemical laboratory.
- will be able to explain chemical nature of selected preparatory techniques. Exercises were chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.
- will have learnt to report thoroughly on outcomes of their work and will have mastered basic chemical calculations needed for their laboratory praxis.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Mgr. Aleš Stýskalík, Ph.D. (seminar tutor)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Tue 11:00–18:50 C10/109, J. Literák, Z. Moravec
C2200/04: Wed 7:00–14:50 C10/109, S. Janků, A. Stýskalík

Prerequisites

C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

The course “Chemical synthesis – laboratory“ represents an elementary laboratory course of preparatory chemistry in bachelor’s studies and aims for deepening and adopting fundamental as well as complementary techniques used in synthetic organic and inorganic chemistry (e.g. vacuum distillation, work under lowered temperatures, column chromatography, synthesis in waterless environment, …) including selected physico-chemical methods for identification of products (determining melting point and refractive index, gas chromatography, IR spectroscopy). Exercises are chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.

Learning outcomes

By the end of this course, students:
- will have mastered elementary and complementary techniques commonly used in inorganic and organic synthesis.
- will be capable of handling laboratory equipment necessary for analysis of purity and identification of prepared solutions with ease (gas chromatograph, IR spectrometer, refractometer, melting point apparatus and others).
- will have built self-confidence and gained manual skillfulness essential for work in chemical laboratory.
- will be able to explain chemical nature of selected preparatory techniques. Exercises were chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.
- will have learnt to report thoroughly on outcomes of their work and will have mastered basic chemical calculations needed for their laboratory praxis.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of benzophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practiced on the real inorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Mgr. Aleš Stýskalík, Ph.D. (seminar tutor)
Mgr. Ondřej Czechaczek (assistant)
Mgr. Martin Kejík, Ph.D. (assistant)
Mgr. Petr Macháč, Ph.D. (assistant)
Mgr. Filip Smrčka, Ph.D. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Thu 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/02: Thu 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/03: Wed 11:00–18:50 C10/109, J. Literák, A. Stýskalík

Prerequisites

( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika || C4221 Biochemical Lab Technique )&& C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

The course “Chemical synthesis – laboratory“ represents an elementary laboratory course of preparatory chemistry in bachelor’s studies and aims for deepening and adopting fundamental as well as complementary techniques used in synthetic organic and inorganic chemistry (e.g. vacuum distillation, work under lowered temperatures, column chromatography, synthesis in waterless environment, …) including selected physico-chemical methods for identification of products (determining melting point and refractive index, gas chromatography, IR spectroscopy). Exercises are chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.

Learning outcomes

By the end of this course, students:
- will have mastered elementary and complementary techniques commonly used in inorganic and organic synthesis.
- will be capable of handling laboratory equipment necessary for analysis of purity and identification of prepared solutions with ease (gas chromatograph, IR spectrometer, refractometer, melting point apparatus and others).
- will have built self-confidence and gained manual skillfulness essential for work in chemical laboratory.
- will be able to explain chemical nature of selected preparatory techniques. Exercises were chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.
- will have learnt to report thoroughly on outcomes of their work and will have mastered basic chemical calculations needed for their laboratory praxis.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Mgr. Petr Macháč, Ph.D. (assistant)
Mgr. Filip Smrčka, Ph.D. (assistant)
Mgr. František Zelenka, Ph.D. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Mon 18. 2. to Fri 17. 5. Tue 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/02: Mon 18. 2. to Fri 17. 5. Tue 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/03: Mon 18. 2. to Fri 17. 5. Mon 8:00–15:50 C10/109, J. Literák, Z. Moravec

Prerequisites

C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of benzophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practiced on the real inorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Mgr. Ondřej Czechaczek (assistant)
Mgr. Petr Macháč, Ph.D. (assistant)
RNDr. Jan Sokolov, Ph.D. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Mon 17. 9. to Fri 14. 12. Thu 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/02: Mon 17. 9. to Fri 14. 12. Thu 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/03: Mon 17. 9. to Fri 14. 12. Wed 11:00–18:50 C10/109, J. Literák, Z. Moravec

Prerequisites

( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika || C4221 Biochemická laboratorní technika )&& C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. At the end the students should master basic methods of preparative organic and inorganic chemistry including identification of the products by selected physico-chemical methods. Students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Mgr. Ondřej Czechaczek (assistant)
Světlana Filípková (assistant)
Mgr. Petra Jarošová, Ph.D. (assistant)
Mgr. Markéta Kandrnálová, Ph.D. (assistant)
Mgr. Svatava Polsterová (assistant)
Mgr. František Zelenka, Ph.D. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Wed 7:00–14:50 C10/109, S. Janků, Z. Moravec
C2200/02: Wed 7:00–14:50 C10/109, S. Janků, Z. Moravec
C2200/03: Thu 8:00–15:50 C10/109, J. Literák, A. Pálková
C2200/04: Thu 8:00–15:50 C10/109, J. Literák, A. Pálková

Prerequisites

C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of benzophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practiced on the real inorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Ing. Ondřej Duda (assistant)
Světlana Filípková (assistant)
RNDr. Jan Sokolov, Ph.D. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Mon 18. 9. to Fri 15. 12. Thu 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/02: Mon 18. 9. to Fri 15. 12. Thu 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/03: Mon 18. 9. to Fri 15. 12. Wed 11:00–18:50 C10/109, J. Literák, Z. Moravec

Prerequisites

( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika || C4221 Biochemická laboratorní technika )&& C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. At the end the students should master basic methods of preparative organic and inorganic chemistry including identification of the products by selected physico-chemical methods. Students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Mgr. Martin Kejík, Ph.D. (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Mon 20. 2. to Mon 22. 5. Tue 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/02: Mon 20. 2. to Mon 22. 5. Tue 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/03: Mon 20. 2. to Mon 22. 5. Wed 8:00–15:50 C10/109, J. Literák, Z. Moravec

Prerequisites

C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of benzophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practiced on the real inorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Ing. Ondřej Duda (assistant)
Světlana Filípková (assistant)
Mgr. Martin Konhefr, Ph.D. (assistant)
Mgr. Tomáš Pastierik (assistant)
RNDr. Jan Sokolov, Ph.D. (assistant)
Mgr. Libor Tanzinger (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Mon 19. 9. to Sun 18. 12. Thu 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/02: Mon 19. 9. to Sun 18. 12. Thu 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/03: Mon 19. 9. to Sun 18. 12. Mon 11:00–18:50 C10/109, S. Janků, Z. Moravec
C2200/04: Mon 19. 9. to Sun 18. 12. Mon 11:00–18:50 C10/109, S. Janků, Z. Moravec

Prerequisites

( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika || C4221 Biochemická laboratorní technika )&& C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. At the end the students should master basic methods of preparative organic and inorganic chemistry including identification of the products by selected physico-chemical methods. Students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Mgr. Martin Kejík, Ph.D. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Thu 7:00–14:50 C10/109, S. Janků, A. Pálková
C2200/02: Thu 7:00–14:50 C10/109, S. Janků, A. Pálková
C2200/03: Tue 8:00–15:50 C10/109, S. Janků, Z. Moravec
C2200/04: Tue 8:00–15:50 C10/109, S. Janků, Z. Moravec

Prerequisites

C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of benzophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practiced on the real inorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
Mgr. Markéta Kandrnálová, Ph.D. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Thu 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/02: Thu 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/03: Wed 11:00–18:50 C10/109, J. Literák, Z. Moravec
C2200/04: Wed 11:00–18:50 C10/109, J. Literák, Z. Moravec

Prerequisites

( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika || C4221 Introductory Biochemistry Laboratory )&& C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. At the end the students should master basic methods of preparative organic and inorganic chemistry including identification of the products by selected physico-chemical methods. Students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Mgr. Tomáš Lízal, Ph.D. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Mon 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/02: Mon 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/03: Tue 8:00–15:50 C10/109, J. Literák, Z. Moravec
C2200/04: Tue 8:00–15:50 C10/109, J. Literák, Z. Moravec

Prerequisites

C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of benzophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practiced on the real inorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Thu 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/02: Thu 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/03: Wed 12:00–19:50 C10/109, J. Literák, Z. Moravec

Prerequisites

( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika || C4221 Introductory Biochemistry Laboratory )&& C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. At the end the students should master basic methods of preparative organic and inorganic chemistry including identification of the products by selected physico-chemical methods. Students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Marie Petlachová, Ph.D. (seminar tutor)
Mgr. Aleš Stýskalík, Ph.D. (seminar tutor)
Světlana Filípková (assistant)
Mgr. Zdeněk Moravec, Ph.D. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Tue 8:00–15:50 C10/109, S. Janků, M. Petlachová
C2200/02: Mon 8:00–15:50 C10/109, J. Literák, M. Petlachová

Prerequisites

C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of benzophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practiced on the real inorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Mgr. Marie Petlachová, Ph.D. (seminar tutor)
Světlana Filípková (assistant)
Mgr. Zdeněk Moravec, Ph.D. (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Thu 7:00–14:50 C10/109, S. Janků, M. Petlachová
C2200/02: Wed 10:00–17:50 C10/109, S. Janků, J. Literák, A. Pálková

Prerequisites

( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika || C4221 Biochemická laboratorní technika )&& C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. At the end the students should master basic methods of preparative organic and inorganic chemistry including identification of the products by selected physico-chemical methods. Students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Mgr. Marie Petlachová, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (assistant)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Tue 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/02: Wed 8:00–15:50 C10/109, J. Literák, A. Pálková

Prerequisites

( C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem. )||( PROGRAM ( B - AB )&& C1020 General Chemistry && C4221 Biochemická laboratorní technika && C4222 Základní laboratorní výpočty )
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potasium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (assistant)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Thu 7:00–14:50 C10/109, S. Janků, A. Pálková
C2200/02: Thu 7:00–14:50 C10/109, S. Janků, A. Pálková
C2200/03: Tue 8:00–15:50 C10/109, J. Literák, A. Pálková
C2200/04: Tue 8:00–15:50 C10/109, J. Literák, A. Pálková

Prerequisites

( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika || C4221 Biochemická laboratorní technika )&& C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 11 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. At the end the students shoudl master basic methods of preparative organic and inorganic chmistry including identification of the products by selected physico-chemical methods. Students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potasium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Mgr. Marie Petlachová, Ph.D. (seminar tutor)
Světlana Filípková (assistant)
Mgr. Zdeněk Moravec, Ph.D. (assistant)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Tue 8:00–15:50 C10/109, S. Janků, M. Petlachová
C2200/02: Wed 9:00–16:50 C10/109, J. Literák, A. Pálková

Prerequisites

( C1100 Introductory Chemistry Lab && C1020 General Chemistry && C1040 General Chemistry-sem. )||( PROGRAM ( B - AB )&& C1020 General Chemistry && C4221 Laboratory techniques in biochemistry && C4222 Basic laboratory calculations )
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 13 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potasium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

( C1100 Introductory Chemistry Lab || C4221 Laboratory techniques in biochemistry )&& C1020 General Chemistry && C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 13 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potasium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Mgr. Marie Petlachová, Ph.D. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Světlana Filípková (assistant)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2200/01: Tue 8:00–15:50 C10/109, S. Janků, A. Pálková
C2200/02: Mon 8:00–15:50 C10/109, J. Literák, M. Petlachová
C2200/03: Wed 10:00–17:50 C10/109, A. Pálková

Prerequisites

( C1100 Laboratorní technika || C1100b Laboratorní technika )&&( C1020 General Chemistry || C1021 General Chemistry )&& C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 140 student(s).
Current registration and enrolment status: enrolled: 0/140, only registered: 0/140, only registered with preference (fields directly associated with the programme): 0/140

fields of study / plans the course is directly associated with

there are 14 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potasium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth. Preparation of chromium(III) oxide and potassium chromate.
  13. Synthesis of ferrocene.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.
Information on course enrolment limitations: Při žádosti o výjimku dostanou přednost studenti programu Chemie a oboru Aplikovaná biochemie

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

The course is not taught in Autumn 2024

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: z (credit).

Teacher(s)

Mgr. Jaroslav Dorošenko, Ph.D. (seminar tutor)
RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
Mgr. Zdeněk Moravec, Ph.D. (seminar tutor)
Mgr. Jan Badin (assistant)
Jaroslav Keller (assistant)
Mgr. Jakub Martikan (assistant)
Ing. Michaela Šusterová (assistant)

Guaranteed by

RNDr. Slávka Janků, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

( C1100 Introductory Chemistry Lab || C1100b Laboratorní technika || C4221 Biochemical Lab Technique )&&( C1020 General Chemistry || C1601 General and Inorg. Chemistry )
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120

fields of study / plans the course is directly associated with

there are 7 fields of study the course is directly associated with, display

Course objectives

The course “Chemical synthesis – laboratory“ represents an elementary laboratory course of preparatory chemistry in bachelor’s studies and aims for deepening and adopting fundamental as well as complementary techniques used in synthetic organic and inorganic chemistry (e.g. vacuum distillation, work under lowered temperatures, column chromatography, synthesis in waterless environment, …) including selected physico-chemical methods for identification of products (determining melting point and refractive index, gas chromatography, IR spectroscopy). Exercises are chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.

Learning outcomes

By the end of this course, students:
- will have mastered elementary and complementary techniques commonly used in inorganic and organic synthesis.
- will be capable of handling laboratory equipment necessary for analysis of purity and identification of prepared solutions with ease (gas chromatograph, IR spectrometer, refractometer, melting point apparatus and others).
- will have built self-confidence and gained manual skillfulness essential for work in chemical laboratory.
- will be able to explain chemical nature of selected preparatory techniques. Exercises were chosen carefully to cover the most common and important types of chemical reactions, which are discussed in lectures on inorganic and organic chemistry, allowing the students to apply their theoretical knowledge in practice.
- will have learnt to report thoroughly on outcomes of their work and will have mastered basic chemical calculations needed for their laboratory praxis.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potassium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

required literature
• LITERÁK, Jaromír, Slávka JANKŮ and Jiří PINKAS. Chemická syntéza - návody k praktiku (Chemical synthesis – practical training). 1. vydání. Brno: Masarykova univerzita, 2012, 139 pp. ISBN 978-80-210-5776-0. info

recommended literature
• PŘÍHODA, Jiří, Miloš ČERNÍK, Slávka JANKŮ and Jaromír LITERÁK. Laboratorní technika. Příručka pro začínajícího chemika (Laboratory technique. Handbook for young chemist). 1. vydání. Brno: Masarykova univerzita, 2012, 221 pp. ISBN 978-80-210-5820-0. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

The course is not taught in Spring 2010

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Slávka Janků, Ph.D. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
Ing. Alena Pálková (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

C1100 Laboratorní technika
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Nomenclature of inorganic and organic compounds. Chemical literature.
  2. Ethyl 3-oxobutanoate ethylenacetale. AN mechanism to C=O, azeotropic and vacuum distillation, work with rotary evaporator.
  3. Synthetic routes to salts. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4. Synthetic routes to acids and halides. Orthoboric acid. Tin(IV) iodide.
  5. 4,4-diphenyl-4-hydroxy-2-butanone ethylenacetale. Extraction, work with rotary evaporator, recrystallization.
  6. Synthetic routes to coordination compounds. Hexaaquacobalt(II) chloride.
  7. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. 3-Nitroacetophenone. SEAr mechanism, recrystallization, IR spectroscopy.
  10. Benzoic acid. AN to C=O, work with anhydrous solvents, extraction, sublimation.
  11. Synthetic routes to oxides. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Ethyl-acetate. Esterifikace, distillation.
  13. 2-Hydroxy-5-methyl-2'-nitroazobenzene. Diazotization and diazonium coupling, recrystallization, TLC.
  14. Final test, make-up class, lab cleaning.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

The information about the term spring 2012 - acreditation is not made public

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)
Mgr. Jaromír Literák, Ph.D. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

( C1100 Laboratorní technika || C1100b Laboratorní technika )&&( C1020 General Chemistry || C1021 General Chemistry )&& C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.
The capacity limit for the course is 120 student(s).
Current registration and enrolment status: enrolled: 0/120, only registered: 0/120, only registered with preference (fields directly associated with the programme): 0/120

fields of study / plans the course is directly associated with

there are 14 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Preparation of orthoboric acid and potasium hydrosulfate.
  2. Preparation of bromoethane. Preparation of bezophenone oxime.
  3. Preparation of ethylmagnesium bromide and its diastereoselective addition to benzoin.
  4. Preparation of 3-nitroacetophenone.
  5. Preparation of 3-aminoacetophenone and 1-(3-nitrophenyl)ethanol.
  6. Preparation of ethyl 3-oxobutanoate ethylenacetal.
  7. Preparation of azo dyes, column chromatography.
  8. Preparation of metal acetylacetonate complexes. Thin-layer chromatography.
  9. Preparation of potassium chlorate. Preparation of hexaaquacobalt(II) chloride.
  10. Preparation of cobalt(III) coordination compounds.
  11. Preparation of boric oxide and trimethyl borate.
  12. Preparation of bismuth(III) oxide and bismuth.
  13. Synthesis of ferrocene.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

The education is realized as a laboratory course, which takes place once a week and the laboratory course covers basic laboratory operations, which are practised on the real anorganic and organic syntheses. In the end the students have to work out the laboratory reports.

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory

Extent and Intensity

0/0/8. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Slávka Janků, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

( C1100 Laboratorní technika || C1100b Laboratorní technika )&&( C1020 General Chemistry || C1021 General Chemistry )&& C1040 General Chemistry-sem.
Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 14 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Nomenclature of inorganic and organic compounds. Chemical literature.
  2. Ethyl 3-oxobutanoate ethylenacetale. AN mechanism to C=O, azeotropic and vacuum distillation, work with rotary evaporator.
  3. Synthetic routes to salts. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4. Synthetic routes to acids and halides. Orthoboric acid. Tin(IV) iodide.
  5. 4,4-diphenyl-4-hydroxy-2-butanone ethylenacetale. Extraction, work with rotary evaporator, recrystallization.
  6. Synthetic routes to coordination compounds. Hexaaquacobalt(II) chloride.
  7. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. 3-Nitroacetophenone. SEAr mechanism, recrystallization, IR spectroscopy.
  10. Benzoic acid. AN to C=O, work with anhydrous solvents, extraction, sublimation.
  11. Synthetic routes to oxides. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Ethyl-acetate. Esterifikace, distillation.
  13. 2-Hydroxy-5-methyl-2'-nitroazobenzene. Diazotization and diazonium coupling, recrystallization, TLC.
  14. Final test, make-up class, lab cleaning.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

C2200 Chemical synthesis - laboratory course

Extent and Intensity

0/0/6. 6 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
prof. Ing. Vladimír Šindelář, Ph.D. (seminar tutor)

Guaranteed by

prof. Ing. Vladimír Šindelář, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of general, inorganic and organic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is offered to students of any study field.

Course objectives

Basic laboratory course in preparative chemistry. Covers syntheses, properties and structures of simple inorganic and organic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Requirements for passing the course. Nomenclature of inorganic and organic compounds. Chemical literature.
  2. Ethyl 3-oxobutanoate ethylenacetale. AN mechanism to C=O, azeotropic and vacuum distillation, work with rotary evaporator.
  3. Synthetic routes to salts. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4. Synthetic routes to acids and halides. Orthoboric acid. Tin(IV) iodide.
  5. 4,4-diphenyl-4-hydroxy-2-butanone ethylenacetale. Extraction, work with rotary evaporator, recrystallization.
  6. Synthetic routes to coordination compounds. Hexaaquacobalt(II) chloride.
  7. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. 3-Nitroacetophenone. SEAr mechanism, recrystallization, IR spectroscopy.
  10. Benzoic acid. AN to C=O, work with anhydrous solvents, extraction, sublimation.
  11. Synthetic routes to oxides. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Ethyl-acetate. Esterifikace, distillation.
  13. 2-Hydroxy-5-methyl-2'-nitroazobenzene. Diazotization and diazonium coupling, recrystallization, TLC.
  14. Final test, make-up class, lab cleaning.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.

Listed among pre-requisites of other courses

• C2720 Organic Chemistry - laboratory course
  (C4221||C1100||C1600)&&!C2200  
• C6190 Advanced laboratory course of inorganic chemistry.
  C2200  

• Enrolment Statistics (Spring 2025, recent)