LA-ICP-MS analysis of metal layers on samples of cultural
heritage

J 2019

LA-ICP-MS analysis of metal layers on samples of cultural heritage

VANÍČKOVÁ, Elena; Markéta HOLÁ; Karel RAPOUCH; David PAVLIŇÁK; Radka KOPECKÁ et al.

Základní údaje

Originální název

LA-ICP-MS analysis of metal layers on samples of cultural heritage

Autoři

VANÍČKOVÁ, Elena; Markéta HOLÁ; Karel RAPOUCH; David PAVLIŇÁK; Radka KOPECKÁ a Viktor KANICKÝ

Vydání

Chemical Papers, Cham, SPRINGER INTERNATIONAL PUBLISHING AG, 2019, 2585-7290

Další údaje

Jazyk

angličtina

Typ výsledku

Článek v odborném periodiku

Obor

10400 1.4 Chemical sciences

Stát vydavatele

Švýcarsko

Utajení

není předmětem státního či obchodního tajemství

Odkazy

Full Text

Označené pro přenos do RIV

Ano

Kód RIV

RIV/00216224:14310/19:00110379

Organizační jednotka

Přírodovědecká fakulta

Klíčová slova anglicky

Laser ablation; Inductively coupled plasma mass spectrometry; Depth profiling; X-ray fluorescence spectroscopy; Metal layer

Štítky

rivok

Příznaky

Mezinárodní význam, Recenzováno

Změněno: 22. 2. 2023 15:26, Mgr. Marie Novosadová Šípková, DiS.

Anotace

V originále

LA-ICP-MS (laser ablation inductively coupled plasma mass spectrometry) was applied as a semi-destructive method for the analysis of metal layers on samples of cultural heritage. The LA system operates at a wavelength of 193 nm with a pulse duration of 4 ns. The laser ablation was performed using spot mode with a diameter of 110 mu m. This method was developed using eight varied reference samples with a defined layer depth and composition. Four real samples of watch cases were analysed, and the layer composition and thickness were determined together with two test reference samples. The analytical results were compared with X-ray fluorescence spectroscopy analysis. The layer thickness was additionally determined by scanning electron microscopy on the cross section of selected samples.

Návaznosti

LO1411, projekt VaV

Název: Rozvoj centra pro nízkonákladové plazmové a nanotechnologické povrchové úpravy (Akronym: CEPLANT plus)

Investor: Ministerstvo školství, mládeže a tělovýchovy ČR, Rozvoj centra pro nízkonákladové plazmové a nanotechnologické povrchové úpravy

LQ1601, projekt VaV

Název: CEITEC 2020 (Akronym: CEITEC2020)

Investor: Ministerstvo školství, mládeže a tělovýchovy ČR, CEITEC 2020

Citovat

VANÍČKOVÁ, Elena; Markéta HOLÁ; Karel RAPOUCH; David PAVLIŇÁK; Radka KOPECKÁ a Viktor KANICKÝ. LA-ICP-MS analysis of metal layers on samples of cultural heritage. Chemical Papers. Cham: SPRINGER INTERNATIONAL PUBLISHING AG, 2019, roč. 73, č. 12, s. 2923-2936. ISSN 2585-7290. Dostupné z: https://doi.org/10.1007/s11696-019-00745-6.

@article{1549042,
   author = {Vaníčková, Elena and Holá, Markéta and Rapouch, Karel and Pavliňák, David and Kopecká, Radka and Kanický, Viktor},
   article_location = {Cham},
   article_number = {12},
   doi = {https://doi.org/10.1007/s11696-019-00745-6},
   keywords = {Laser ablation; Inductively coupled plasma mass spectrometry; Depth profiling; X-ray fluorescence spectroscopy; Metal layer},
   language = {eng},
   issn = {2585-7290},
   journal = {Chemical Papers},
   title = {LA-ICP-MS analysis of metal layers on samples of cultural heritage},
   url = {https://link.springer.com/article/10.1007/s11696-019-00745-6},
   volume = {73},
   year = {2019}
}

TY  - JOUR
ID  - 1549042
AU  - Vaníčková, Elena - Holá, Markéta - Rapouch, Karel - Pavliňák, David - Kopecká, Radka - Kanický, Viktor
PY  - 2019
TI  - LA-ICP-MS analysis of metal layers on samples of cultural heritage
JF  - Chemical Papers
VL  - 73
IS  - 12
SP  - 2923-2936
EP  - 2923-2936
PB  - SPRINGER INTERNATIONAL PUBLISHING AG
SN  - 25857290
KW  - Laser ablation
KW  - Inductively coupled plasma mass spectrometry
KW  - Depth profiling
KW  - X-ray fluorescence spectroscopy
KW  - Metal layer
UR  - https://link.springer.com/article/10.1007/s11696-019-00745-6
L2  - https://link.springer.com/article/10.1007/s11696-019-00745-6
N2  - LA-ICP-MS (laser ablation inductively coupled plasma mass spectrometry) was applied as a semi-destructive method for the analysis of metal layers on samples of cultural heritage. The LA system operates at a wavelength of 193 nm with a pulse duration of 4 ns. The laser ablation was performed using spot mode with a diameter of 110 mu m. This method was developed using eight varied reference samples with a defined layer depth and composition. Four real samples of watch cases were analysed, and the layer composition and thickness were determined together with two test reference samples. The analytical results were compared with X-ray fluorescence spectroscopy analysis. The layer thickness was additionally determined by scanning electron microscopy on the cross section of selected samples.
ER  -

VANÍČKOVÁ, Elena; Markéta HOLÁ; Karel RAPOUCH; David PAVLIŇÁK; Radka KOPECKÁ a Viktor KANICKÝ. LA-ICP-MS analysis of metal layers on samples of cultural heritage. \textit{Chemical Papers}. Cham: SPRINGER INTERNATIONAL PUBLISHING AG, 2019, roč.~73, č.~12, s.~2923-2936. ISSN~2585-7290. Dostupné z: https://doi.org/10.1007/s11696-019-00745-6.

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