ŽÍDEK, Lukáš, Haihong WU, Juli FEIGON a Vladimír SKLENÁŘ. Measurement of small scalar and resiudal dipolar couplings in purine and pyrimidine bases. Journal of Biomolecular NMR. Dordrecht: Kluwer/Escom, 2001, roč. 21, č. 2, s. 153-159. ISSN 0925-2738. |
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@article{375591, author = {Žídek, Lukáš and Wu, Haihong and Feigon, Juli and Sklenář, Vladimír}, article_location = {Dordrecht}, article_number = {2}, keywords = {NMR methods; nucleic acid bases; residual dipolar couplings; spin-state-selective filter}, language = {eng}, issn = {0925-2738}, journal = {Journal of Biomolecular NMR}, title = {Measurement of small scalar and resiudal dipolar couplings in purine and pyrimidine bases}, volume = {21}, year = {2001} }
TY - JOUR ID - 375591 AU - Žídek, Lukáš - Wu, Haihong - Feigon, Juli - Sklenář, Vladimír PY - 2001 TI - Measurement of small scalar and resiudal dipolar couplings in purine and pyrimidine bases JF - Journal of Biomolecular NMR VL - 21 IS - 2 SP - 153 EP - 153 PB - Kluwer/Escom SN - 09252738 KW - NMR methods KW - nucleic acid bases KW - residual dipolar couplings KW - spin-state-selective filter N2 - A suite of spin-state-selective excitation (S3E) NMR experiments for the measurements of small one-bond (13C - 13C, 13C - 15N) and two-bond (1H - 13C, 1H - 15N) coupling constants in 13C, 15N labeled purine and pyrimidine bases is presented. The incorporation of band-selective shaped pulses, elimination of the cross talk between á and â sub-spectra, and accuracy and precision of the proposed approach are discussed. Merits of using S3 E rather than á/â-half-filter are demonstrated using results obtained on isotopicaly labeled DNA oligonucleotides. ER -
ŽÍDEK, Lukáš, Haihong WU, Juli FEIGON a Vladimír SKLENÁŘ. Measurement of small scalar and resiudal dipolar couplings in purine and pyrimidine bases. \textit{Journal of Biomolecular NMR}. Dordrecht: Kluwer/Escom, 2001, roč.~21, č.~2, s.~153-159. ISSN~0925-2738.
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