Course Information

C2100 Inorganic Chemistry - laboratory course

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2100/01: Mon 13:00–19:50 C10/312, M. Černík
C2100/02: Tue 7:00–13:50 C10/312, A. Pálková
C2100/03: Wed 13:00–19:50 C10/312, A. Pálková

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2100/01: Wed 14:00–20:50 C10/312, J. Novosad
C2100/02: Thu 13:00–19:50 C10/312, J. Pinkas
C2100/03: Mon 13:00–19:50 C10/312, Z. Spíchal
C2100/04: Fri 11:00–17:50 C10/312, M. Nečas
C2100/05: Tue 7:00–13:50 C10/312, A. Pálková
C2100/06: Tue 14:00–20:50 C10/312, M. Černík
C2100/07: Wed 7:00–13:50 C10/312, A. Pálková

Prerequisites

Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 20 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why specialist techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Assessment methods

The course can also be completed outside the examination period. The course is taught annually. The course is taught: every week.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
Ing. Jitka Halvová (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
Mgr. Marie Petlachová, Ph.D. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)
Mgr. Martin Vyšvařil, Ph.D. (seminar tutor)
Světlana Filípková (assistant)

Guaranteed by

doc. RNDr. Josef Novosad, CSc.
Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2100/01: Tue 14:00–19:50 C10/312, M. Černík
C2100/02: Mon 14:00–19:50 C10/312, J. Novosad
C2100/03: Wed 7:00–13:50 C10/312, A. Pálková
C2100/04: Wed 14:00–19:50 C10/312, J. Pinkas
C2100/05: Tue 7:00–13:50 C10/312, J. Halvová, M. Petlachová
C2100/06: Thu 7:00–13:50 C10/312, J. Halvová, M. Vyšvařil
C2100/07: Mon 7:00–13:50 C10/312, J. Halvová, Z. Spíchal
C2100/08: Fri 9:00–15:50 C10/312, M. Nečas

Prerequisites

Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 21 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Assessment methods (in Czech)

Laboratorní cvičení probíhá každý týden. V úvodní hodině cvičení je probráno obecné téma přípravy některé ze základních tříd anorganických sloučenin. V následujícím cvičení jsou znalosti probraného tématu a také absolvovaných cvičení zkontrolovány testem. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny rovnice a výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena (omluvenky předány na studijní oddělení) a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
RNDr. Aleš Mareček, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
RNDr. Richard Ševčík, Ph.D. (seminar tutor)
RNDr. Jan Taraba, Ph.D. (seminar tutor)

Guaranteed by

doc. RNDr. Josef Novosad, CSc.
Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2100/01: Fri 14:00–19:50 03016, M. Nečas
C2100/02: Mon 7:00–13:50 03016, J. Taraba
C2100/03: Tue 14:00–19:50 03016, A. Mareček
C2100/04: Wed 14:00–19:50 03016, D. Dastych
C2100/05: Thu 7:00–13:50 03016, M. Černík
C2100/06: Thu 14:00–19:50 03016, J. Novosad
C2100/07: Wed 7:00–13:50 03016, J. Křivohlávek
C2100/08: Mon 14:00–19:50 03016, J. Křivohlávek
C2100/09: Fri 7:00–13:50 03016, R. Ševčík

Prerequisites

Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 21 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Assessment methods (in Czech)

Laboratorní cvičení probíhá každý týden. V úvodní hodině cvičení je probráno obecné téma přípravy některé ze základních tříd anorganických sloučenin. V následujícím cvičení jsou znalosti probraného tématu a také absolvovaných cvičení zkontrolovány testem. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny rovnice a výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena (omluvenky předány na studijní oddělení) a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
RNDr. Jan Taraba, Ph.D. (seminar tutor)

Guaranteed by

doc. RNDr. Josef Novosad, CSc.
Department of Chemistry – Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2100/01: Wed 7:00–13:50 03016, J. Křivohlávek
C2100/02: Thu 14:00–19:50 03016, J. Taraba
C2100/03: Tue 13:00–19:50 03016, D. Dastych
C2100/04: Fri 7:00–13:50 03016, M. Nečas
C2100/05: Wed 14:00–19:50 03016, M. Černík
C2100/06: Tue 7:00–13:50 03016, J. Novosad

Prerequisites

Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 21 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate, alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Potassium oxalate monohydrate, manganometric titration. Iron(II) sulfate.
  3. Copper(II) sulfate, copper(I) iodide. Mohr's salt.
  4. Synthetic routes to oxides. Orthoboric acid.
  5. Chromium(III) oxide. Potassium chomate. Purity assessment of Mohr's salt.
  6. Synthetic routes to hydroxides. Hexaaquacobalt(II)chloride. Potassium tris(oxalato)chromate(III).
  7. Hexaaminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to acids. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to salts. Potassium chlorate. .
  11. Boric oxide, trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Synthetic routes to halides. Potassium disulfate, potassium methylsulfate.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Synthetic routes to coordination compounds. Potassium peroxydisulfate. Iodometric titration.

Literature

• Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info

Assessment methods (in Czech)

Laboratorní cvičení probíhá každý týden. Každý druhý týden je v úvodní hodině cvičení probráno jedno obecné téma přípravy některé ze základních tříd anorganických sloučenin. V následujícím cvičení jsou znalosti probraného tématu zkontrolovány testem. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny rovnice a výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
RNDr. Jan Taraba, Ph.D. (seminar tutor)

Guaranteed by

doc. RNDr. Josef Novosad, CSc.
Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2100/01: Tue 14:00–19:50 03016, M. Nečas
C2100/02: Wed 7:00–12:50 03016, J. Křivohlávek
C2100/03: Thu 14:00–19:50 03016, D. Dastych
C2100/04: Fri 7:00–12:50 03016, J. Taraba
C2100/05: Wed 14:00–19:50 03016, M. Černík
C2100/06: Fri 13:00–18:50 03016, M. Nečas

Prerequisites

Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 21 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate, alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Potassium oxalate monohydrate, manganometric titration. Iron(II) sulfate.
  3. Copper(II) sulfate, copper(I) iodide. Mohr's salt.
  4. Synthetic routes to oxides. Orthoboric acid.
  5. Chromium(III) oxide. Potassium chomate. Purity assessment of Mohr's salt.
  6. Synthetic routes to hydroxides. Hexaaquacobalt(II)chloride. Potassium tris(oxalato)chromate(III).
  7. Hexaaminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to acids. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to salts. Potassium chlorate. .
  11. Boric oxide, trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Synthetic routes to halides. Potassium disulfate, potassium methylsulfate.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Synthetic routes to coordination compounds. Potassium peroxydisulfate. Iodometric titration.

Literature

• Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info

Assessment methods (in Czech)

Laboratorní cvičení probíhá každý týden. Každý druhý týden je v úvodní hodině cvičení probráno jedno obecné téma přípravy některé ze základních tříd anorganických sloučenin. V následujícím cvičení jsou znalosti probraného tématu zkontrolovány testem. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny rovnice a výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

Extent and Intensity

0/0/6. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Milan Alberti, CSc. (seminar tutor)
RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
RNDr. Jan Taraba, Ph.D. (seminar tutor)

Guaranteed by

doc. RNDr. Josef Novosad, CSc.
Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2100/01: No timetable has been entered into IS. J. Taraba
C2100/02: No timetable has been entered into IS. D. Dastych
C2100/03: No timetable has been entered into IS. M. Černík
C2100/04: No timetable has been entered into IS. J. Křivohlávek
C2100/05: No timetable has been entered into IS. J. Novosad
C2100/06: No timetable has been entered into IS. M. Nečas

Prerequisites

Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 21 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate, alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Potassium oxalate monohydrate, manganometric titration. Iron(II) sulfate.
  3. Copper(II) sulfate, copper(I) iodide. Mohr's salt.
  4. Synthetic routes to oxides. Orthoboric acid.
  5. Chromium(III) oxide. Potassium chomate. Purity assessment of Mohr's salt.
  6. Synthetic routes to hydroxides. Hexaaquacobalt(II)chloride. Potassium tris(oxalato)chromate(III).
  7. Hexaaminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to acids. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to salts. Potassium chlorate. .
  11. Boric oxide, trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Synthetic routes to halides. Potassium disulfate, potassium methylsulfate.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Synthetic routes to coordination compounds. Potassium peroxydisulfate. Iodometric titration.

Literature

• Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info

Assessment methods (in Czech)

Laboratorní cvičení probíhá každý týden. Každý druhý týden je v úvodní hodině cvičení probráno jedno obecné téma přípravy některé ze základních tříd anorganických sloučenin. V následujícím cvičení jsou znalosti probraného tématu zkontrolovány testem. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny rovnice a výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

Study Materials
The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Milan Alberti, CSc. (seminar tutor)
RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
RNDr. Aleš Mareček, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2100/01: No timetable has been entered into IS. D. Dastych
C2100/02: No timetable has been entered into IS. J. Pinkas
C2100/03: No timetable has been entered into IS. M. Alberti
C2100/04: No timetable has been entered into IS. M. Černík
C2100/05: No timetable has been entered into IS. J. Novosad
C2100/06: No timetable has been entered into IS. M. Nečas
C2100/07: No timetable has been entered into IS. J. Křivohlávek

Prerequisites

Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

there are 21 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate, alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Potassium oxalate monohydrate, manganometric titration. Iron(II) sulfate.
  3. Copper(II) sulfate, copper(I) iodide. Mohr's salt.
  4. Synthetic routes to oxides. Tin(IV) iodide. Orthoboric acid.
  5. Chromium(III) oxide. Potassium chomate. Purity assessment of Mohr's salt.
  6. Synthetic routes to hydroxides. Hexaaquacobalt(II)chloride. Potassium tris(oxalato)chromate(III).
  7. Hexaaminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to acids. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to salts. Potassium chlorate. Pentaammine-nitrocobalt(III) chloride and pentaammine-nitritocobalt(III) chloride.
  11. Boric oxide, trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Synthetic routes to halides. Potassium disulfate, potassium methylsulfate. Vacuum sublimation of SnI4.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Synthetic routes to coordination compounds. Potassium peroxydisulfate. Iodometric titration.

Literature

• Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info

Assessment methods (in Czech)

Laboratorní cvičení probíhá každý týden. Každý druhý týden je v úvodní hodině cvičení probráno jedno obecné téma přípravy některé ze základních tříd anorganických sloučenin. V následujícím cvičení jsou znalosti probraného tématu zkontrolovány testem. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny rovnice a výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

Extent and Intensity

0/7/0. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Milan Alberti, CSc. (seminar tutor)
RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
RNDr. Aleš Mareček, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Radek Sluka, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Chemistry Section – Faculty of Science

Timetable of Seminar Groups

C2100/A: No timetable has been entered into IS. J. Pinkas
C2100/B: No timetable has been entered into IS. J. Novosad
C2100/C: No timetable has been entered into IS. M. Alberti
C2100/D: No timetable has been entered into IS. R. Sluka
C2100/E: No timetable has been entered into IS. M. Černík
C2100/F: No timetable has been entered into IS. D. Dastych
C2100/G: No timetable has been entered into IS. D. Dastych

Prerequisites

Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate, alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Potassium oxalate monohydrate, manganometric titration. Iron(II) sulfate.
  3. Copper(II) sulfate, copper(I) iodide. Mohr's salt.
  4. Synthetic routes to oxides. Tin(IV) iodide. Orthoboric acid.
  5. Chromium(III) oxide. Potassium chomate. Purity assessment of Mohr's salt.
  6. Synthetic routes to hydroxides. Hexaaquacobalt(II)chloride. Potassium tris(oxalato)chromate(III).
  7. Hexaaminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to acids. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to salts. Potassium chlorate. Pentaammine-nitrocobalt(III) chloride and pentaammine-nitritocobalt(III) chloride.
  11. Boric oxide, trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Synthetic routes to halides. Potassium disulfate, potassium methylsulfate. Vacuum sublimation of SnI4.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Synthetic routes to coordination compounds. Potassium peroxydisulfate. Iodometric titration.

Assessment methods (in Czech)

Laboratorní cvičení probíhá každý týden. Každý druhý týden je v úvodní hodině cvičení probráno jedno obecné téma přípravy některé ze základních tříd anorganických sloučenin. V následujícím cvičení jsou znalosti probraného tématu zkontrolovány testem. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny rovnice a výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru. Podmínky pro zápočet jsou: odevzdání všech preparátů v dostatečném množství a čistotě, úplné a pečlivé zápisy v laboratorním deníku o provedených reakcích a experimentech včetně výpočtů, znalosti principů všech procvičených úloh, vlastností připravených látek, stechiometrických a zřeďovacích výpočtů a výpočtů titrací.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

Extent and Intensity

0/7/0. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Milan Alberti, CSc. (seminar tutor)
RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
RNDr. Aleš Mareček, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
doc. RNDr. Antonín Růžička, CSc. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Chemistry Section – Faculty of Science

Prerequisites (in Czech)

C1061 Inorganic Chemistry I

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Course objectives

Basic inorganic course Part II. This part covers syntheses, properties and structures of compounds of groups V-VIII.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé katedry anorganické chemie.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

Extent and Intensity

0/7/0. 8 credit(s). Type of Completion: graded credit.

Teacher(s)

RNDr. Milan Alberti, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
RNDr. Aleš Mareček, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
doc. RNDr. Antonín Růžička, CSc. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Chemistry Section – Faculty of Science

Prerequisites (in Czech)

C1061 Inorganic Chemistry I

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

there are 18 fields of study the course is directly associated with, display

Syllabus

• Basic inorganic course Part II. This part covers syntheses, properties and structures of compounds of groups V-VIII.

Language of instruction

Czech

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé katedry anorganické chemie.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2025

Extent and Intensity

0/0/7. 7 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2024

Extent and Intensity

0/0/7. 7 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2023

Extent and Intensity

0/0/7. 7 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2022

Extent and Intensity

0/0/7. 7 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2021

Extent and Intensity

0/0/7. 7 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2020

Extent and Intensity

0/0/7. 7 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2019

Extent and Intensity

0/0/7. 7 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in spring 2018

Extent and Intensity

0/0/7. 7 credit(s). Type of Completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2017

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2016

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2015

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2014

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2013

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2012

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2011

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
RNDr. Aleš Mareček, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
RNDr. Richard Ševčík, Ph.D. (seminar tutor)
RNDr. Jan Taraba, Ph.D. (seminar tutor)

Guaranteed by

doc. RNDr. Josef Novosad, CSc.
Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 21 fields of study the course is directly associated with, display

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Assessment methods (in Czech)

Laboratorní cvičení probíhá každý týden. V úvodní hodině cvičení je probráno obecné téma přípravy některé ze základních tříd anorganických sloučenin. V následujícím cvičení jsou znalosti probraného tématu a také absolvovaných cvičení zkontrolovány testem. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny rovnice a výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena (omluvenky předány na studijní oddělení) a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé katedry anorganické chemie.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in spring 2012 - acreditation

The information about the term spring 2012 - acreditation is not made public

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

C2100 Inorganic Chemistry - laboratory course

The course is not taught in Spring 2011 - only for the accreditation

Extent and Intensity

0/0/7. 7 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).

Teacher(s)

RNDr. Miloš Černík, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science

Prerequisites

c1620 General and Inorg.Chem.-lab. || c1080 General Chemistry-lab.course
Basic knowledge of general and inorganic chemistry. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing will be used extensively.

Course Enrolment Limitations

The course is only offered to the students of the study fields the course is directly associated with.

fields of study / plans the course is directly associated with

• Applied Biochemistry (programme PřF, B-AB)
• Biochemistry (programme PřF, B-BCH)
• Chemistry (programme PřF, B-CH)

Course objectives

Basic laboratory course in inorganic preparative chemistry. Covers syntheses, properties and structures of simple inorganic compounds, such as oxides, halides and other salts, acids and their functional derivatives, and complexes. At the end of the course students should be able to explain the principles that underpin selected synthetic processes, and why special techniques are required for their preparation.

Syllabus

• 1. Introduction, safety rules, laboratory notebook, worked example of experiment calculations. Potassium hydrogen sulfate. Alkalimetric titration.
  2. Preparative route selection criteria. Solubility. Precipitation reactions. Iron(II) sulfate.
  3. Synthetic routes to oxides. Copper(II) sulfate. Copper(I) iodide. Mohr's salt.
  4.. Synthetic routes to oxides and hydroxides. Orthoboric acid. Tin(IV) iodide.
  5. Synthetic routes to acids. Chromium(III) oxide. Potassium chromate. Purity assessment of Mohr's salt.
  6. Synthetic routes to acids. Hexaaquacobalt(II) chloride. Purity assessment of potassium chromate.
  7. Synthetic routek to salts. Hexaamminecobalt(III) chloride. Pentaammine-chlorocobalt(III) chloride. Potassium tetraperoxochromate(V).
  8. Synthetic routes to salts. Metal acetylacetonate complexes. Thin-layer chromatography.
  9. Synthetic routes to halides. Calcium tungstate. Crystal structures of basic inorganic compounds.
  10. Synthetic routes to halides. Potassium chlorate. Pentaammine-nitritocobalt(III) chloride. Pentaammine-nitrocobalt(III) chloride.
  11. Synthetic routes to coordination compounds. Boric oxide. Trimethylborate. Amonnium tetrathiomolybdate(VI).
  12. Potassium disulfate. Potassium methylsulfate. Vacuum sublimation of tin(IV) iodide.
  13. Bismuth(III) oxide. Bismut. Thermite reaction.
  14. Potassium peroxydisulfate. Iodometric titration. Alkalimetric titration.

Literature

• Masarykova univerzita. Přírodovědecká fakulta. Návody ke cvičení z anorganické chemie. Brno, Masarykova univerzita, 2006, 80 s.
• KLIKORKA, Jiří. Úvod do preparativní anorganické chemie. 3. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974, 373 s. info
• TANAKA, John and Steven L. SUIB. Experimental Methods in Inorganic Chemistry. New Jersey: Prentice Hall, 1999, 393 pp. ISBN 0-13-841909-4. info

Teaching methods

Laboratory course covers preparations of selected inorganic compounds and keeping of the lab notebook. Laboratory course runs on a weekly basis. In the first part of the class period, a general topic of the preparation of some basic class of inorganic comounds is discussed. Regular tests of students knowledge by short written tests are carried out at the beginning of the class. Students are required to present all equations, calculations, and procedure schemes in their laboratory notebooks before the class onset. Missed classes must be made up by the end of semester.

Assessment methods

The course is completed by graded credits. Quality of laboratory notebook, yields of syntheses, and purity of products are evaluated and graded. Regular tests of students knowledge by short written tests and questions.

Language of instruction

Czech

Follow-Up Courses

• C5380 Special Laboratory Techniques
• C6190 Advanced laboratory course of inorganic chemistry.

Further comments (probably available only in Czech)

The course is taught annually.
The course is taught: every week.

Listed among pre-requisites of other courses

• Bi4020c Molecular biology - laboratory practice
  (C1600 || C1080 || C1620 || C1650 || C2100 || C2500 || C2740 || C2480 || Bi9410 || souhlas) && (Bi4020 || NOW(Bi4020)) && !NOWANY(Bi4010c,Bi4035) && !Bi4010c && !Bi4035  

• Enrolment Statistics (recent)